烧结温度对Ba2LaBiO6_ZnO复相材料的微观形貌和电性能的影响.pdfVIP

机械工程师

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烧结温度对BaLaBiO/ZnO复相材料的26

微观形貌和电性能的影响

罗彦琦，张锦荣

（东莞理工学院城市学院智能制造学院，广东东莞523419）

摘要：

通过选取ZnO掺杂AlO的固溶体材料为低阻相，BaLaBiO材料为高B值高阻相制备复相材料，研究原料成分、烧

2326

结温度对材料的晶相组成、微观形貌和电性能的影响规律，利用XRD和SEM进行分析，并获取可靠的制备工艺参数。试验

结果显示：BaLaBiO/ZnO复相材料体系具有明显的NTC（负温度系数）性能，材料的最佳烧结温度为1050～1100℃。随着

26

5

烧结温度的升高，样品的晶粒尺寸增大，材料趋向致密，呈现规则的几何形状。室温电阻率籽由1000℃的8.65×10Ω·cm

25

4

减小到1100℃的1.35×10Ω·cm，材料的B系数值基本不变。