The Effect of Stirring Rate on the Detection of Hydrogen Peroxide for Carbon Paste Electrode Modified with Meldola’s Blue.pptVIP

下载本文档

3
0
约 1页
2017-09-29 发布于山西
举报
版权申诉

The Effect of Stirring Rate on the Detection of Hydrogen Peroxide for Carbon Paste Electrode Modified with Meldola’s Blue.ppt

1、本文档共1页，可阅读全部内容。
2、原创力文档（book118）网站文档一经付费（服务费），不意味着购买了该文档的版权，仅供个人/单位学习、研究之用，不得用于商业用途，未经授权，严禁复制、发行、汇编、翻译或者网络传播等，侵权必究。
3、本站所有内容均由合作方或网友上传，本站不对文档的完整性、权威性及其观点立场正确性做任何保证或承诺！文档内容仅供研究参考，付费前请自行鉴别。如您付费，意味着您自己接受本站规则且自行承担风险，本站不退款、不进行额外附加服务；查看《如何避免下载的几个坑》。如果您已付费下载过本站文档，您可以点击这里二次下载。
4、如文档侵犯商业秘密、侵犯著作权、侵犯人身权等，请点击“版权申诉”（推荐），也可以打举报电话：400-050-0827(电话支持时间：9:00-18:30)。
5、该文档为VIP文档，如果想要下载，成为VIP会员后，下载免费。
6、成为VIP后，下载本文档将扣除1次下载权益。下载后，不支持退款、换文档。如有疑问请联系我们。
7、成为VIP后，您将拥有八大权益，权益包括：VIP文档下载权益、阅读免打扰、文档格式转换、高级专利检索、专属身份标志、高级客服、多端互通、版权登记。
8、VIP文档为合作方或网友上传，每下载1次，网站将根据用户上传文档的质量评分、类型等，对文档贡献者给予高额补贴、流量扶持。如果你也想贡献VIP文档。上传文档

* * The Effect of Stirring Rate on the Detection of Hydrogen Peroxide for Carbon Paste Electrode Modified with Meldola’s Blue Chi-Wen Lo (羅濟玟) , Chih-Ying Wu (巫致穎) , Hau Lin (林浩) Department of Chemical and Materials Engineering, Southern Taiwan University 南台科技大學化學工程與材料工程系 ABSTRACT . A study was conducted to use the Meldola’s Blue to modify the carbon paste electrode. Because the Meldola’s Blue possesses the excellent catalytic characteristic, it can be used with the graphite carbon powders which possesses the excellent conductivity to make the carbon paste electrode and to elevate the responding current of hydrogen peroxide. The responding current of hydrogen peroxide is detected in the phosphate buffer solution(PBS) and then the concentration of the hydrogen peroxide can be obtained and consequently, the concentration of the glucose can be determined. At 30℃, -300 mV operating potential, and in 0.05 M phosphate buffer solution (PBS), the TB (Time Base) graphs for the carbon paste electrode at different stirring rates were plotted to evaluate the effect of stirring rates on the responding current of detection of hydrogen peroxide. At the optimum operating conditions -300 mV operating potential, 500 rpm stirring rate and in 0.05 M PBS buffer solution ( pH = 7.4 ) , when the carbon paste electrode was modified with Meldola’s Blue [Meldola’s Blue : carbon powders : carbon paste = 2 ：15 ：15 ( weight ratio )] , the detection limit was 0.02 mM H2O2 , the linear range was 0.02～1.4 mM H2O2 , R2 = 0.9994 , the sensitivity was 159.39 μA/cm2．mM H2O2. Because hydrogen peroxide is used in the food industry for the purpose of preservation occasionally, a rapid and convenient hydrogen peroxide sensor for detection of the hydrogen peroxide is an important research subject. In recent years, diabetes has become one of the top ten causes of death for the people in Taiwan and therefore developing a rapid and convenient glucose biosensor also has become an