沉淀法制备钨酸铅纳米粉体.pdfVIP

硅 酸 盐 学 报 34 5 Vol. 34 No. 5 第 卷第 期 2006 5 May 2006 年 月 JOURNAL OF THE CHINESE CERAMIC SOCIETY 沉淀法制备钨酸铅纳米粉体沉淀法制备钨酸铅纳米粉体 沉淀法制备钨酸铅纳米粉体沉淀法制备钨酸铅纳米粉体 1 2 2 1. 烟台大学环境和材料工程学院 山东 烟台 264005 2. 山东大学 晶体材料国家重点实验室 济南 250100 摘摘 要要 以钨酸钠和硝酸铅为原料 以聚乙二醇 为分散剂 用沉淀法配制出钨酸铅混浊液 将钨酸铅混浊液在 烘干后 制备出钨酸铅纳米 摘摘 要要 200 100 粉体 对制备的样品进行 射线衍射分析 结果表明 钨酸铅纳米粉体结晶良好 将制备的样品在不同温度退火后 用透射电镜分析了其形貌 结 X 果表明 钨酸铅纳米粉体的颗粒粒度随着退火温度的升高而增大 关键词关键词 钨酸铅 沉淀法 纳米粉体 关键词关键词 中图分类号中图分类号 O614.43 文献标识码文献标识码 A 文章编号文章编号 0454–5648(2006)05–0601–03 中图分类号中图分类号 文献标识码文献标识码 文章编号文章编号 PREPARATION OF LEAD TUNGSTATE NANO-PARTICLES BY DEPOSITION METHOD WANG Zhuo1 YANG Yuguo2 YANG Changhong2 (1. School of Environment and Materials Engineering, Yantai University, Yantai 264005, Shandong; 2. State Key Laboratory of Crystal Materials, Shandong University, Jinan 250100, China) Abstract: Lead tungstate nano-particles were prepared by deposition after being heat-treated at 100 , using lead nitrate and natrium tungstate as starting materials and polyglycol 200 as dispersant. The XRD pattern indicates that the well crystalized lead tungstate nano-particles were obtained under the given synthesis conditions. The prepared nano-particles were heat-treated at different temperatures. Transmission electron microscopy was used to study their morphologies. The results show