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Low temperature sintering characteristics and
properties of SOFC ceramic interconnect material
1
La0.7Ca0.3Cr0.97O3
Songlin Wang，Xingqin Liu, Guangyao Meng
Department of Materials Science and Engineering, University of Science and Technology of China
(USTC), Hefei (230026) P.R. China
E-mail ：wsl@
Abstract
Relatively low temperature (1150-1300 ℃) sintering characteristics and electric conductivities of
La Ca Cr O with a slight Cr deficiency of 0.03 ，prepared by an auto-ignition process, have been
0.7 0.3 0.97 3
discussed. The material could reach 94.3 % relative density at 1200 °C for 5 h in air, which is about
200 ℃ lower than that of with no Cr deficiency. XRD results indicated that pure perovskite phase was
formed after sintered at the temperature range of 1150-1300℃. The sample sintered at 1250 °C had the
maximum conductivity of 62.0 Scm-1 at 850 °C in air, which is about 2.6 times as high as that of
La Ca CrO with no Cr deficiency. In pure H , it got the maximum electrical conductivity of 3.3
0.7 0.3 3 2
Scm-1 at 850 °C as sintered at 1200 °C. The TEC of the material was about 11.4 × 10-6 K-1, which is
very compatible to that of other common used SOFC components. Therefore, it is a simple and
cost-effective interconnect material for SOFCs.
Keywords: Lanthanum chromite; Cr deficiency; Auto-igniti
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