花椒籽仁油脱酸_脱蜡精制工艺研究_殷钟意.pdfVIP

20 10 35 10 15 1 1 1 1 2 殷钟意, 杜若愚, 刘方丹, 郑旭煦 , 汤 敏 ( 1重庆工商大学 环境与生物工程学院, 废油资源 技术与装备教育部工程研究中心, 重庆 400067; 2綦江县环境保护局, 重庆 40 14 20 ) : 通过比较酸 - 碱炼- 结晶法和酸 - 碱炼- 溶剂法对花椒籽仁油的脱蜡效果, 选择酸 - 碱炼- 结晶法精制花椒籽仁油以脱蜡率为指标, 重点考察了结晶温度结晶时间氢氧 钾浓度 对脱蜡效果的影响通过正交试验确定的酸 - 碱炼- 结晶法的最佳工艺条件为: 结晶温度 8 , 结晶时间 8 h, 氢氧 钾浓度 0 5 mo l/L在最佳条件下花椒籽仁油的脱蜡率为 82 28% , 脱酸率为 97 20% : 花椒籽仁油; 脱酸; 脱蜡 : TQ 644 4; TS224 6 : A : 1003- 7969 ( 2010) 10 - 0015 - 03 Deacidification and dewaxing of Ch inese prick ly ash kernel oil 1 1 1 1 2 Y IN Zhongy i, DU Ruoyu , L IU F angdan , ZH ENG Xuxu , TANG M in ( 1Eng ineering R esearch Center o fW aste O il R ecovery T echnology and Equ ipm ent, M in istry of Edu cat ion, Co llege o f Env ironm ent and B ioeng ineering, Chongq ing T echnology and Bu siness U n iversity, Chongqing 4000 67, China; 2Env ironm enta l Pro tection A gency of Q ijiang C ounty, Chongqing 401420, Ch ina) Abs tract: Phosphoric acid re fin ing - alka li ref in ing - crystalliza tion w as comp ared w ith phospho ric ac id re fin ing- alkali refining- so lven t extraction in the dew ax ing effect o f Ch inese prickly ash kernel o il, and the m ethod of phosphoric acid refining - a lkali ref in ing - crystallization w as choosed The in flu ence o f crysta llization tem p erature, crysta llizat ion t mi e and concentration o f po tassium hydrox ide on the dew ax ing rat io w as investiga ted The resu lts of orthogonal exp ermi ent show ed th at the optmi a l cond ition