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One dimensional ZnO nanostructured films Effect of oxide nanoparticles教程.pdf

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Materials Letters 82 (2012) 13–15 Contents lists available at SciVerse ScienceDirect Materials Letters journal h omepage: /locate/matlet One-dimensional ZnO nanostructured ﬁlms: Effect of oxide nanoparticles T. Frade, M.E. Melo Jorge, A. Gomes ⁎ CCMM, Department of Chemistry and Biochemistry, University of Lisbon, Campo Grande C8, 1749-016 Lisbon, Portugal a r t i c l e i n f o a b s t r a c t Article history: ZnO nanorods were prepared on ﬂuorine doped tin oxide (FTO) using the electrodeposition method. The ar- Received 8 February 2012 chitecture of the ZnO nanorods arrays was strongly modiﬁed by addition of TiO2 nanoparticles during the Accepted 10 May 2012 electrodeposition process. Scanning electron microscopy (SEM) and X-ray diffraction (XRD) were used to Available online 17 May 2012 characterize their morphology and structure and conﬁrmed the successful formation of ZnO nanorods. The ZnO-TiO2 modiﬁed electrodes demonstrated an increase of the photocurrent activity under enhanced UV Keywords: Zinc oxide white light irradiation. This was attributed to the increased surface area and therein the photoactive surface Nanostructures area. Modiﬁed electrode © 2012 Elsevier B.V. All rights reserved. Electrodeposition 1. Introduction