硫铁矿炼磺渣选铁还原焙烧磁选还原剂试验的研究.docVIP

硫铁矿炼磺渣选铁还原焙烧磁选还原剂试验研究 刘金浪，张桂芳，张宗华，张 昱 (昆明理工大学，云南 昆明 650093) 摘要：根据炼磺渣的性质，采用预选抛尾的方法预选了试样，在此基础上，分另日进行了预选粗精矿还原焙烧的还原20min，温度在850℃时.还5%、还原剂粒度以mm、磁场强度以0.29 T为宜，得到的铁品位为51.71%，铁回77.20%。 ：硫铁矿炼磺渣；还原焙烧；还原剂；磁选 Experiment on reducing agent for recovering iron from pyrite sulfur refining slag by reduction roasting and magnetic separation LIU Jin-lang, ZHANG Gui-fang, ZHANG Zong-hua, ZHANG Yu (Kunming University of Science and Technology, Kunming Yunnan 650093, China) Abstract: According to the nature of refining sulfur residue, the samples were selected by the pre-concentration to reject tailing. On this basis, the experiments of reduction roasting of the pre-concentration crude concentrate were done, including these experiments of the sort of reducing reagent, the dosage of reducing reagent, the granularity of reducing agent, and magnetic field strength. Results showed that when the time of pre-coarse concentrate roasting lasted 20 minutes at 850 C, the sort of suitable reducing agent was the coke, and the dosage of suitable reducing agent was 5%, and the granularity of suitable reducing agent was - 1ram, and the suitable magnetic field strength was 0.29 T, and the iron grade of 51.71% and the iron recovery of 77.20 % were obtained. Keywords: pyrite sulfur refining slag; reduction masting; reducing agent; magnetic separation 0 引言 硫磺烧渣中一般含有低于20%的铁，属于低20%。该类烧渣的[2-8]。1 研究方法 1.1 试样性质 试样是四川某硫铁矿炼磺渣，化学成分分析1。 表1 试样主要化学成分分析结果 % 此外还对试样进行了光谱分析和试样铁物相 1.2 试验方案 由于原矿品位较低，采用预选抛尾的方法得32.24%的预选产品后，根据铁矿的性质，1 mm，采0.1 T的磁场强度进行选别。还原剂用量试验1%、3%、5%、8%四种不同的用量；还原剂0.5、1+0.5、1、2+1、3+2 mm五个不同粒级。 2 研究结果与讨论 2.1 原矿还原焙烧还原剂种类试验 焙烧条件：时间20 min、温度850℃、还原剂5%、粒度1 mm、弱磁选磁场强度0.1 T，0.074 mm占90%以上。试验结2。2 还原剂种类试验结果 从表2看出，无烟煤做还原剂得到的磁性产24.84%，铁品位为53.19%，铁回收率为61.08%的铁精矿选矿指标。 2.2 预选粗精矿还原焙烧还原剂用量试验 焙烧条件：时间20 min，温度850℃，焦炭用1%、3%、5%、8%，焦炭粒度mm。弱磁选0.1 T，磁选物料细度0.074 mm占90%以上。试验结果见图1。图1 还原剂用量试验结果 从图1看出，还原剂用量太少，还原气氛不5%为好。 2.3 预选粗精矿还原焙烧还原剂粒度试验 试验条件：还原焙烧时间20 min，温度855%，焦炭粒度0.5、1+0.5、1、2+1、3+2 mm，弱磁选磁场强度0