实验#2：二茂铁和醯二茂铁.docVIP

实验#2:二茂铁和乙醯二茂铁 WARNING NOTICE: The experiments described in these materials are potentially hazardous and require a high level ofsafety training, special facilities and equipment, and supervision by appropriate individuals. You bear the sole responsibility, liability, and risk for the implementation of such safety procedures and measures. MIT shall have no responsibility, liability, or risk for the content or implementation of any of the material presented. Legal Notices 警告：在这些数据中所描述的实验是有潜在危险的，而且要求有高度的安全训练、特别的设施和装备，且要有适当的人员监督下才能进行的。你要独自承担责任， 义务，而且要为履行上述的安全手续和措施负责。麻省理工学院将没有责任，义务，或是为满足上述材料提及到的安全措施而负责。法律说明 MASSACHUSETTS INSTITUTE OF TECHNOLOGY Department of Chemistry 5.310 Laboratory Chemistry 麻省理工学院 化学系 5.310化学实验 EXPERIMENT #2 THE PREPARATION OF FERROCENE AND ACETYLFERROCENE 实验#2 二茂铁和乙醯二茂铁的制备 PURPOSE AND BACKGROUND OF THE EXPERIMENT I.实验的目的和背景 The principal aims of this experiment are: 实验的主要目的是: 1. To provide experience in the synthesis of a relatively simple covalent compound, bis(pentahaptocyclopentadienyl) iron, (η5-C5H5)2Fe, whose trivial name is ferrocene (1). 1. 为合成一个相对简单的共价化合物,二环茂二烯基铁, (η5-C5H5)2Fe,它的俗名是二茂铁(1) 2. To become familiar with inert atmosphere techniques. 2. e熟悉惰性气氛技术 3. To introduce the use of thin-layer chromatography as an analytical tool and Last Assignment: Negotiation Take Aways 15.665 Power and Negotiation Sloan School of Management I. Negotiation Take Aways as Corporate Capability (1-2 pages, double-spaced) A. Select and Industry, Firm or Job i. Select an industry, firm or job of interest ii. Describe one (1) typical negotiation situation in that industry/firm/job. 1. What are the characteristics of these negotiation situations in terms of their distributive/integrative potential, emotional content, likelihood of future interaction with counterparts, etc. 2. Are these negotiations likely to be with counterparts that are internal and/or external to a firm, teams, etc. iii. Develop a set of recommendations for a one or t