Simultaneous Determination of Bisphenols and Alkylphenols in Water by Solid Phase Extraction and Ultra Performance Liquid Chromatography-tandem Mass Spectrometry.pdfVIP

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Simultaneous Determination of Bisphenols and Alkylphenols in Water by Solid Phase Extraction and Ultra Performance Liquid Chromatography-tandem Mass Spectrometry.pdf

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Simultaneous Determination of Bisphenols and Alkylphenols in Water by Solid Phase Extraction and Ultra Performance Liquid Chromatography-tandem Mass Spectrometry.pdf

BiomedEnvironSci，2014；27(6)：471—474 471 LettertotheEditor SimultaneousDeterminationofBisphenolsandAlkylphenols inW aterbySolidPhaseExtractionandUltraPerformanceLiquid Chromatography·tandem MassSpectrometry SHAN XiaoMei她 SHEN DengHui一，WANG BingShuang，LU BeiBei，andHUANG FaYuan ， To establish an analyticaI method for industriaIapplications ，arestartingtobeusedfor determinationoffourbisphenols(BPA，BPB，BPF， the production of epoxy resins． However． no andBPS)andtwoalkylphenols(4一n-OP，4-n—NP)in maximum residue levels ormigration limits have waterbyultraperformanceliquidchromatography- been establishedto dateforthese compoundsin tandem massspectrometry (UPLC／MS／MS)．The water．In recentyears’research，thesecompounds watersampleswereextractedandcondensedwith alsohavebeenfoundanestrogenicactivitysim iIarto solid—phaseextraction(SPE)usingCl8cartridgesand BPA ．ItispossibletoreleaseofBPsandAPsinto eluted byacetonitrile．Separationwascarriedout the environment during manufacturing and by with Acquity BEH C8column and detection were Ieachingfr0m finalproducts．So．thedetermination performed byUPLC／MS／MS．Quantification was of these compounds in environmenta1 water calculated byusingthe internaIstandard BPA-dl6 sampies is demanded for environmentaI risk and4一n-NP．d8．Thelinearcorrelationcoe仟icientsof assessment．ThetraceleveIc0ncentratiOnofthese thesecompoundsintherangeof1．0-100．0I~g／L contaminants and the cornplex matrix in were allover 0．999．The minimum detectable environmenta1water sampies makes it usualIY c0ncentrati0ns were 0．75—1．0 ng／L． and the necessarytopretreatbeforeinstrumentaIanaIysis． recoveriesranged from 87．0％ to 106．9％．Relative MethodsforanaIyzing BPsand APsinwater standa