样品形状对直读光谱分析结果的影响_吴金龙.pdfVIP

* ( 315800) 3 mm 4 mm 6 mm 8 mm 10 mmC Si Mn P S Cr Ni Mo Cu V 2 mmCr Mo 12 mm 8 mm 6 mm 4 mm 3 mm C Mn P S Cr Ni Cu Si Mo V 4334 The Effect of Shape of Specimens on the Results with Direct-Reading Spark Spectrometry Wu Jinlong, Chao Xiaofang, Zhao Ting, Huang Shijie, Jin Xianzhong* (Beilun Entry-Exit Inspection and Quarantine Bureau, Ningbo, Zhejiang, 315800) Abstract: The effect of the width of narrow strip specimens, diameter and slant-endedness of round-bar specimens on the results with direct-reading spark spectrometry was investigated. Strip specimen, whose width was 3 mm, 4 mm, 6 mm, 8 mm, 10 mm respectively, was spliced and analyzed; The results of C, Si, Mn, P, S, Cr, Ni, Mo, Cu, V were acceptable, then the results of Cr, Mo obviously changed to the 2 mm specimen. Round-bar specimens, which their diameters were Φ25 mm, Φ12 mm, Φ8 mm, Φ6 mm, Φ4 mm and Φ3 mm, were analyzed; their results indicated that with the specimen diameter becoming smaller, the element result of C, Mn, P, S, Cr, Ni, Cu became bigge