改性凹土对银杏叶总黄酮的静态吸附性能研究.pdfVIP

※基础研究 食品科学 2010, Vol. 31, No. 17 47 改性凹土对银杏叶总黄酮的静态吸附性能研究 尹秀莲，游庆红 (淮阴工学院生命科学与化学工程学院，江苏淮安 22300 1) 摘 要：采用改性凹土吸附银杏叶总黄酮，通过对4 种不同改性凹土的筛选，发现壳聚糖改性凹土对银杏叶总黄 酮有较大的吸附量，为112 .70mg/g ；对壳聚糖改性凹土对银杏叶总黄酮的吸附性能进行研究，得到溶液总黄酮质 量浓度、p H 值对吸附量的影响趋势曲线、吸附等温线、吸附动力学曲线及吸附速率曲线；以解吸率、总黄酮纯 度为指标对洗脱剂进行选择，发现1% 乙酸-7 0 % 乙醇溶液洗脱较好，解吸率为9 1% ，纯度为5 6 % 。 关键词：改性凹凸棒土；银杏叶总黄酮；吸附性能 Static Adsorption Properties of Total Flavonoids from Ginkgo biloba Leaves on Modified Attapulgite Clay YIN Xiu-lian ，YOU Qing-hong , (School of Life Science and Chemical Engineering, Huaiyin Institute of Technology, Huai an 22300 1, China) 　　　　　　　　　　　　　 Abstract ：Modified attapulgite clay as an adsorbent was used to explore the adsorption properties of the total flavonoids from Ginkgo biloba leaves. Four different kinds of modified attapulgite clay were investigated for their adsorption capacities towards the total flavonoids, and chitosan-modified attapulgite clay was found to have the largest adsorption capacity, which was up to 112.70 mg/g. The adsorption properties of the total flavonoids on chitosan-modified attapulgite clay were explored, and the curves showing the respective effects of sample concentration and pH on the adsorption capacity of the total flavonoids on chitosan- modified attapulgite clay and the adsorption isothermal curves and kinetic curves were plotted. The optimal desoprtion solvent for achieving both high desorption rate (9 1%) and total flavonoid purity (56%) was composed of 70% ethanol and 1% acetic acid. Key words ：modified attapulgite clay ；total flavonoids from Ginkgo biloba leaves ；adsorption properties 中图分类号：R284 .2 文献标识码：A 文章编号：1002-6630(20 1