侧链型聚醚改性氨基硅的合成及应用.pdfVIP

279 精 细 化 工 Vol. 27, No. 9 2 0 1 0 9 FINE CHEM ICALS Sep t. 2 0 1 0 * 黄 洁, 安秋凤 , 黄良仙, 丁 洋 ( , 71002 1) : 0150~ 1800 Pa , 0200~ 0596 mm ol/ g, n20 1656 7~ 1668 5, d ( SPEAS) : 60~ 100 ! , 4 1 ~ 8 h FT IR, HNMR TEM , , 20% SPEAS (), , 148 : ; ; : TQ 340. 4; O634. 4 : A : 1003- 5214( 2010) 09- 0903- 05 Synthesis andApplication of Sidechain PolyethercontainingAminopolysiloxane * HUANG Jie, AN Q iufeng , HUANG L iangx ian, D ING Yang (K ey Laboratory of A ux iliary Chem istry and Techno logy f or Chem ical Industry, M inistry of Education, Shaanx i Uni ersity of Science and Technology, X i∀an 7 10021, Shaanx i, China) Abstract:The w aterolub le polyethercontain ing am inopoly iloxane( SPEAS) w a ynthe ized. It v i 20 co ity, am ino value and nd w ere 0150 ~ 1800 Pa , 0200 ~ 0596 mm ol/ g and 1656 7 ~ 1668 5. The optmi um condition w ere reaction tem perature 60~ 100 ! , reaction tmi e 4~ 8 h. Then 1 the tructure and propertie of the am ple w ere analyzed by FT IR, HNMR and TEM. Expermi ental re ult how ed that the ize of the particle of uch aqueou di per ion at 20% w ere different. The bending rig idity of the treated fabric decrea ed ( the oft handfeeling enhanced), it w ri