雷公藤和昆明山海棠化学成分相似性分析.pdfVIP

安徽农业科学 ,Journal of Anhui Agri . Sci . 2009 ,37 ( 13) :5961 - 5963 　　　　　　　　　　　　　　　　　责任编辑 　李玮 　责任校对 　况玲玲 雷公藤和昆明山海棠化学成分相似性分析 (桂林医学院 ,广西桂林 541004) 黄耀峰 , 沈雪松 , 顾生玖 , 朱开梅 , 李芳耀 　 摘要　[ 目的]研究雷公藤和昆明山海棠化学成分的相似性 。[ 方法]采用乙醚、氯仿和乙酸乙酯等有机溶剂对雷公藤和昆明山海棠植物 根茎进行顺序热提取 。其提取液经浓缩后对相对应部位进行薄层层析检查、化学成分的预测和熔点的测定来判别 2 种植物的差异 。 [ 结果] 结果表明,2 种植物含有很多相似的化学成分 。其薄层层析法的检查结果可作为雷公藤和昆明山海棠植物的生药鉴定 , 以及判断 质量的指标 。[ 结论] 该研究结果对进一步分离、提纯雷公藤及昆明山海棠所含的化学成分及研究各化学成分的结构有一定的参考 作用 。 关键词　雷公藤; 昆明山海棠; 化学成分鉴别; 薄层层析法 ( ) 中图分类号　S661.4 　　文献标识码　A 　　文章编号　0517 - 6611 2009 13 - 05961 - 03 Analysis on Similarity of Chemical Compositions of bet ween Tripterygium wilfordii Hook. f . and Tripterygium hypoglaucum ( Lévl . ) Hutchins ( ) HUANG Yaofeng et al 　 Guilin Medical University , Guilin , Guangxi 541004 Abstract 　 [Obj ective ] The purpose of this research was to study the similarity of chemical composition of Tripterygium wifl ordii Hook .f . and Triptery gium hypoglaucum (Lévl . ) Hutchins. [Method ] The chloroform , ethyl acetate and other organic solvents were used for root extraction under heat sequence in this essay . After concerntration of the extract , TLC examination , prediction of chemical composition and melting point determination were applied for j udgement between the two plants’differences. [ Result ] The results showed that the two species contained a lot of similar chemical composition . The ex perimental results of TLC examination could be regarded as pharmacognostic identification , quality standard of tripterygium and THH. [ Conclusion ] This research will give some references in the further separation , purification , compositions and chemical structure study of Tripterygium wifl ordii Hook .f . and Tripterygium hypoglaucum