亚麻籽中氰化物定性定量方法的研究.pdfVIP

Vo .l 29, N o. 06, 2008 1, 2 2 , ( 11湖南省农产品加工研究所, 湖南长沙 410125; 21江南大学食品学院, 江苏无锡 214122) :建立测定亚麻籽中氰化 的定性定量方法结果表明,改进的异烟酸-吡唑啉酮比色法能进行亚麻籽氰化 2 的测定,检测方法具有很强的线性相关性, R = 019986, 加标回收率 93108%~ 95165%, 相对标准偏差 5%本方法灵 敏,准确可靠,重现性好, 测定的结果可靠 :亚麻籽,生氰糖苷, 氰化 , 测定 S tudy on qua litative and quantitative methods of cyan ide in flaxseed 1, 2 2 L I G ao- yang , D ING X iao- lin ( 11Institute ofHunan griculturalProduct Processing, Changsha 410125, China; 21SchoolofFood Science andTechnology, JiangnanUniversity,W uxi 214122, China) A bstract: Ob jective to estab lish a qualitative and quantitativem ethods ofcyanide ni flaxseed1 Results showed that mod ified isonicotine ac id- pyrazolone colorm etric method was possible to measure cyanide content of flaxseed, 2 w ith very strong linear relevance ( R = 019986) and hgi h returns- ratio of add itive sample ( 93108%~ 95165% ) as wellas sm all relative standard deviation ( less than 5% ) 1 The methods were sens itive, accurate, reliab le, and suitab le for the detection of cyanide1 Key wo rds: flaxseed; cyanog enic glycoside; cyanide; measurem ent : TS20715 : : 1002-0306( 2008) 06-0291-03 , , , , :( HCN)[ 5mg/kg, ( X- 3 X- 6) 5mg/kg[9] ) ) ) , , [ 1, 2] [ 10] , , , ,