分批萃取精馏回收无水乙醇的新工艺_胡晖.pdfVIP

26 6 现代化工 Ju e 2006 2006 6 Moder Chemical I dustry # 53 # 分批萃取精馏回收无水乙醇的新工艺 1,2 3 2 1,2 胡 晖 , 邬慧雄, 徐世民, 李鑫钢 ( 1. 天津大学化工学院, 天津300072; 2. 天津大学精馏技术国家工程研究中心, 天津300072; 3. 清华大学化学工程系, 北京100084) : , , , , , : ; ; ; ; :TQ028. 8;TQ2231122 :A : 0253- 4320( 2006) 06- 0053- 03 Study on batch extractive distillation for ethanol purification 1, 2 1 2 1 , 2 H U Hui , WUH ui-x iong , X U Shi-min , LI X in-gang ( 1. School of Chemical E gi eeri g a dTech ology, Tia ji U iversity, Tia ji 300072, Chi a; 2. Natio al E gi eeri g Research Ce ter for Distillatio Tech ology, Tia ji U iversity, Tia ji 300072, Chi a; 3. Chemical E gi eeri g Departme t, Tsi ghua U iversity, Beiji g 100084, Chi a) Abstract: A ew correspo di g optimal revampi g for batch extractive distillatio ( BED) i etha ol purificatio , which adds a reboiler a d a additio al storage ta k,was put forward. I the ew modificatio , the liquid from the bottom of the tower directly flows i to the additio al ta k, so the liquid volume i distilli g still does pt i crease duri g the whole process of BED. Mea time, i this ew mode, the varyi g degree of reboiler temperature becomes smaller, a d the heati g co trol becomes easier, a d the operati g time becomes shorter. It is possibly useful to the modificatio of BED for etha ol purificatio . Key words: extractive distillatio ; etha ol; ethyle e glycol; reclamatio ; a hydrous etha ol , , ,