铂催化-非散射红外吸收法测定过氧化氢中总有机碳.pdfVIP

2007 4 17 4 C h inese Jou nal of H ea lth Labo ato y T echnology, Ap 2007; V ol 17 No 4 645 铂催化- 非散射红外吸收法测定过氧化氢中的总有机碳 王春娥, 潘振球, 鲁兵, 李剑 ( , 410005) [ ] : : , : , , , : 01m g/kg: [ ] 过氧化氢; 铂; 催化; 总有机碳; 测定 [ ] O 6573 [] A [ ] 1004- 8685( 2007) 04- 0645- 02 P latinum catalysis- ND IR m ethod for detecting total organic carbon in hydrogen p erox ide products W ang Chune, P an Zhenqiu, L u B ing, L i J ian ( H unan Cente fo D isease Cont o l and P evention, Changsha 410005, China) [ Abstract] O bjective T o establish a m ethod fo detecting to ta l o ganic ca bon in hyd ogen pe ox ide p oductsM ethod s A fte hyd ogen pe ox ide p oducts w e e ca talyzed by p la tinum, to tal o gan ic ca bon in itw as detected by ND IRR esults Samp le - p epa a tion w as s mi p leThe esu ltw as accu ate and e liab leThe detec tion lmi itw as 01m g/kgConc lusion The m ethod is su itab le fo dete m ination of to tal o gan ic ca bon in hyd ogen pe ox ide p oducts [ K ey words] H yd ogen pe ox ide; P latinum; C ata lyze; T ota l o gan ic ca bon; D etect 12 仪器与试剂 [ 2] , , 121 仪器 1010 TO C, O - I- A na lg tica l , , 122 试剂 TOC [, ( , C) = 1 000 mg /L ]; 5% ( V /V ) ; 100 g/L ; , ; , , 13 测定方法 , 131 仪器条件 : 038~ 042 M P a; , : 25 m ;l : 400 ;l : , , 1 500 l; T IC: 2 m in; TOC : 25 m in; T IC , : 1 m in; TOC: 15 m in; : 25