分子蒸馏分离超临界CO_2萃取的米藁精油及其成分分析.pdf

24 10 精 细 化 工 V o .l 24, No. 10 2 0 0 7 10 FINE CHEM ICALS O ct. 2 0 0 7 CO 2 * 1, 2 1 1 2 李天祥 , 朱 静 , 曾祥钦 , 王静康 ( 1. , 550003; 2. , 300072) : , CO , 2 , 12 GC- M S, 98, 44, , , 2007 4 301178 : ; ; ; ; : R 2842; O 2421 : A : 1003- 5214( 2007) 10- 0984- 04 UsingM olecular D istillation to Separate EssentialO il Extracted from M igao y Supercritical CO and Its Component Analysis 2 1, 2 1 1 2 L T ian-x iang , ZHU Jing , ZENG X iang-qin , WANG J ing-kang (1. School of Chemical Engineering and Technology, Guizhou University, Guiyang 550003, Guizhou, China; 2. School of ChemicalEngineering and Technology, Tianjin University, Tianj in 300072, China) A stract:M o lecular d istillation(MD) w as used to separate the essential o il ex tracted by supercritica l CO2 flu id ex traction ( SFE) from Cinnamomum igaoH. W. Li(M igao) , and 12 fractionsw ere obta ined at different evaporating tem peratures and pressures. ts com ponents were analyzed by GC - M S and 98 com pounds w ere identified in tota,l in wh ich, 44 com pounds, such as va lencene and to rreyo,l w ere ident ified for the first t mi e in the fractions