共沉淀法合成NdYAG粉体及pH值的影响.pdfVIP

· 陶瓷 · 33 H值的影响‘ 共沉淀法合成Nd：YAG粉体及p 刘智勇1 温文嫫2 庞 驰1 (1贵州大学材料与冶金学院贵阳 550003)(2内蒙占工业大学理学院呼和浩特010051) 摘要 粉体的成分和性能影响显著．当pH值为8．0时．前驱粉末在1000℃热处理2h后．全部转化成纯YAG相．粉体产生软团 聚．主要为层状结构。并伴有小量纳米颗粒。 关键词 Nd：YAG透明陶瓷共沉淀法 Powder Methodand theEffectof PreparationNd：YAG byCo—precipitationStudy pH Liu Chil(1TheMaterialsand ofGuizhou Zhiyon91，WenWenyin92。Pang MetallurgyCollege (2ScienceofInner of MongoliaUniversityTechnology．Hohhot．010051) were the method Abstract：Ndo．∞Y2．97A15012(Nd：YAG)powderspreparedby homogeneousco—precipitationusingYz()3、 AI(N()3)3·9H2()andNd(N03)3asrawmaterials．7lheammoniumcarbonateas calcined hydrogen precipitator．Thepow— ders e— werecharacterizedthe anddifferential diffraction。and by thermogravimetryscanningcalorimetry．X—ray scanning lectron the of of cubic value．Itisshownthat：whenthe value Nd：YAG microscope．researchimpactpH pH 8．0。pure pow— derswereobtained the l 2 haveasoft by precursorat 000℃forh．The Nd：YAG agglomerate． calcining prepared powders structureis asmallamountof 1ayered mainly．andaccompaniedby nano—particles． KeyWords：Nd：YAG；Transparentceramics；Co—precipitationmethod； 简单，易操作，制备周期短、成本低，易于实现工业化批 前言 量生产。