《Effect of Draw Ratio on the Morphologies and Properties of BPDAPMDAODA Polyimide Fibers》.pdfVIP
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Chem.Res.Chin.Univ.,2014,30(1),163—167
EffectofDrawRatioonthe and of
MorphologiesProperties
BPDA/PMDA/ODAFibers
Polyimide
ZHANG 1”,ZHANG Yanhu3,LIGuomin2,LIU
Chunling Qion91”,XUE Fangfan92,QIUXuepengp,
andGAOLianxun‘
儿Xianglin93
Scienceand
ofMaterials 130025,PR.China;
,.College Engineering,JilinUniversity,Changchun
2.PolymerCompositeEngineeringLaboratory,
3.State and Institute
Key Physics Chemistry,
LaboratoryofPolymer Chemistry,ChangchunofApplied
Chinese 130022,尸R.China
AcademyofSciences。Changchun
Abstract
3,3,4,4.Biphenyltetracarboxylicdianhydride/pyromellitic
fiberswithdifferentdrawratioswere fromtheimidizationof
ODA)polyimidecopolymer prepared polyacrylic
viaa
acid(PAA)fibersdry-jetwet-spinningprocess.Theirmorphologies,microcrystalorientations,thermalstabilities,
andmechanical were via electron diffrac—
propertiesinvestigatedscanning microscopy(SEM),wideangleX—ray
tensile orderto fiberswithbetterme-
tion(WAXD),thermogravimetricanalysis(TGA),andexperiments.Inacquire
chanical aimedat the draw thermalimidizationresultedina
performance.weob
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