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利用乙炔炭黑薄膜修饰电极的α萘乙酸电化学检测
目 录
摘要
1、中文摘要··························································2
2、英文摘要·························································3
一、前言···································································4
1、α-萘乙酸························································4
2、玻碳电极···························································4
3、薄膜修饰电极····················································5
4、乙炔炭黑和双十六烷基磷酸····································5
5、电极反应过程····················································6
6、研究目的·························································7
二、实验部分·····························································7
1、试剂·······························································7
2、实验仪器··························································7
3、乙炔炭黑薄膜修饰电极的制备······································7
4、分析步骤··························································8
三、结果与讨论··························································8
1、AB / DHP薄膜修饰GCE的电化学的行为····························8
2、NAA的电化学行为··················································9
3、扫描频率的影响····················································10
4、AB／DHP悬浮液的量的影响·········································10
5、富积时间的影响····················································11
6、可重复性和再生性···············································11
7、线性范围和检测极限············································12
8、干扰试验·························································12
9、分析应用·························································13
四、结论·································································13
五、参考文献····························································13
六、致 谢································································15
利用乙炔炭黑薄膜修饰电极
的α-萘乙酸电化学检测
中文摘要：通过超声波振荡，将乙炔碳黑（AB）分散在双十六烷基磷酸溶液（DHP）中,形成稳定的分散均匀的AB/DHP悬浮液。蒸发掉水分之后，即得到AB/DHP混合薄膜修饰电极。以裸电极时对K3[Fe( CN)6]的响应为基准，观测DHP修饰电极与AB/DHP薄膜修饰电极。结果发现AB/DHP薄膜修饰电极有大的表面积，以及具有电子迁移速率恒定不变的特性，此外，检测α-萘乙酸（NAA）在电极上的电化学行为，发现在AB/DHP薄膜修饰电极上α-萘乙酸
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