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PAPER /jaas | Journal of Analytical Atomic Spectrometry
In situ Nd isotopic analysis of geological materials by laser ablation
MC-ICP-MS
Gavin L. Foster* and Derek Vance
Received 3rd October 2005, Accepted 25th January 2006
First published as an Advance Article on the web 9th February 2006
DOI: 10.1039/b513945g
Neodymium (Nd) isotopes have widespread applications in the earth sciences, both in
geochronology and in provenance/tracer studies. The isotopic analyses are conventionally done by
chemical separation of pure Nd from the sample matrix. This process is time consuming and loses
potentially vast amounts of information held at small spatial scales. Here, we describe a laser
ablation protocol for the measurement of Nd isotopes in geological materials with relatively high
Nd concentrations ( Z 100 ppm; e.g., apatite, titanite, and ferromanganese nodules). The
procedure allows, for the first time, the exploitation of information held in Nd isotopes at scales
of less than 0.1 mm. The principal analytical issues to be overcome are the interferences from
isobaric Sm isotopes, the correction for which must be very accurate in order to maintain a high
accuracy for the Nd isotopic ratios. We show that careful attention to mass discrimination effects
along with an iterative correction procedure allows a correction that results in an accuracy on the
143Nd/144Nd isotope ratio of the order of 0.5 epsilon units (0.005%) for Sm/Nd ratios as high as
1.2. The total analysis time is short (B2–5 min), enabling a large number of analyses (30) in
each analytical session. Spatial resolution is governed by the Nd concentration and the required
accuracy and for apatites and titanites it is typically B90 mm. Analytical precision is degraded by
around a factor of 2–3 relative to the best TIMS and solution MC-ICP-MS data. Crucially,
however, the rapid sample throughput and the extremely high spatial
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