响应面设计分析法在金属矿物微波处理中的应用.docVIP

应用响应面设计分析法研究碳酸锰吸收微波的性能 马少健1，梁玉石2，封金鹏1，莫伟1，苏秀娟1 (1. 广西大学 资源与冶金学院，南宁 530004；2. 广西大学 环境学院，南宁 530004) 摘要：以碳酸锰为微波吸收材料，考察了微波输出功率、微波辐射时间、样品堆积厚度和样品质量等因素对微波吸收率的影响。基于单因素条件影响试验结果，采用响应面法进行试验设计、方差分析、曲面分析及模型优化。结果表明，各因素影响显著程度为：微波功率样品堆积厚度样品质量辐射时间，且交互影响不显著。当微波功率为675 W、作用时间为131.5 s、样品堆积厚度为15.4 mm、样品质量为153.6 g时，碳酸锰的微波吸收率模拟值最优为6.28%，与实际试验结果（5.89%）能较好吻合，误差约为6.6%。响应面分析法对矿物微波处理过程的因素影响程度有较好的预测性。 关键词：微波；碳酸锰；响应面设计分析法 中图分类号：TB34 文献标识码：A 文章编号：1007-7545（2012）02-0000-00 Study on Microwave Absorbing Property of Manganese Carbonate Using Response Surface Methodology MA Shao-jian1, LIANG Yu-shi2, FENG Jin-penga1, MO Wei1, SU Xiu-juan1 (1. College of Resources and Metallurgy, Guangxi University, Nanning 530004, China; 2. School of Environment, Guangxi University, Nanning 530004, China) Abstract：Manganese carbonate was used as microwave absorbing material. The effects of microwave power, treating time, thickness, and mass of samples on microwave energy absorption rate were investigated. Based on single factor experimental results, response surface methodology(RSM) was adopted to design the optimized experiments, analyze the variance and curved surfaces, and to optimize the parameters of fitted mathematical model. The simulated results indicated that the significant level of factors were microwave power, thickness, mass of samples and treating time in order, respectively. The interaction between two of these factors was not significant. The optimized conditions were found as: microwave power was 675 W, time was 131.5 s, thickness was 15.4 mm, mass of samples was 153.6 g. Under these conditions, the predicted absorption rate reached 6.28% by the fitted model, while the actual experimental value was about 5.89% with small relative error to the former. Therefore, it showed that response surface design and its analysis had a good predicted performance in microwave treatment process of minerals. Key words：microwave; manganese carbonate; response surface methodology 近年来，微波加热作为一种清洁高效的加热技术在矿冶领域已经开始受到广泛研究，主要