催化剂制备和表征 英文.ppt

TPR, TPD, TPO, and TPSR Temperature Programmed Reduction, Desorption, Oxidation, and Surface Reaction (TPR/TPD/TPO/TPSR). 1-H2 and N2 mixed gases; 2-silica gel dryer; 3-deoxidant; 4-mass flow meter; 5-temperature controller; 6-heater; 7-quartz reactor; 8-catalyst sample; 9-TCD; 10-thermocouple; 11-condenser; 12-recorder. H2-TPR profile of Ni(383)/S-1273 after reaction for 100 h H2-TPR profiles of different catalyst samples (a) Ni(383)/S-1273; (b) Ni(383)/S-823; (c) Ni(823)/S-1273; (d) Ni(823)/S-823; (e) Ni(1273)/S-823. NH3-TPD to detect the acid sites on catalyst surface NH3-TPD profiles of