4,X射线衍射方向课题.pptVIP

*;*;*;*;*;*;*;*;*;*;*;*;*;*;由劳厄方程推导Bragg方程 ;*;反射条件： I k– k0 I = I K I = 1/dhkl = 2 sinq/l，得Bragg方程 l = 2 d sinq ;*;*;*;*;*;*;*;*;*;*;*;*;*;*;*;*;*;粉末多晶样品的倒易空间特点;粉末多晶样品的倒易空间特点;粉末多晶样品的倒易空间特点;In order to record a proper powder pattern, the sample should be rotated or more grains should be added. The middle image shows a 2D diffraction pattern obtained from 200 grains. The corresponding 1D trace along [h00] (red curve) shows a much better representation of the intensities. Still some of the reflections do not show the correct intensity. ;Experimental Powder Diffraction ;*;*;*;*;*;*