气质联用法测定溶性纺织助染剂中氯化甲苯化合物.docVIP

气质联用法测定水溶性纺织助染剂中氯化甲苯化合物 摘 要：建立了剂的气相色谱-质谱（GC-MS）测定方法。程序升温方式进行测定结果表明该方法对种的回收率%～%，方法检测限～μg/kg。该法，适用于中的分析。 关键词：chlorinated toluenes in water-soluble textile dyeing auxiliary via GC-MS method Abstract：A testing method for determination of chlorinated toluenes in water-soluble textile dyeing auxiliary with GC-MS was established. With ultrasonic-assisted the sample was extracted twice by n-hexane. Then the extract was analyzed with DB-17MS by the temperature programming mode of GC-MS and was tested by external standard method. The results showed that with this method satisfactory recoveries 81.9%～%