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Basically,no serious effect of aggregation of particles on the determining results of primary particle size PCS method Primary particles Granulation Secondary particle SAXS method ZnSe Granulation The different kind of samples Nano-particles dispersed in plastic membrane Mesochannel molecular sieve Nano-particles dispersed in steel Magnetic liquid Polyamide membrane γ-Al O 2 3 Periodical zone,Random Zone CAT-1 CAT-2 CAT-2 Pore size distribution Cat-2 Pore size distribution TiN dispersed in a steel particle An extruded powder stainless steel Particle size distribution of TiN extracted from the steel Magnetic liquid in a magnetic filed Data treatment test report 寻峰操作 1 2 3 减小此值峰增多 Y表示软件寻到的峰所在的位置 1 3 2 寻找组分 1 2 1 2 左键点住拖动 标准卡片峰强及峰位 实验卡片峰强及峰位 右键 标准谱图 实验谱图 无任何元素限制搜索卡片的结果 左键拖动 随意拖动一个峰不全重合时的情况 Y表示未对上的峰 转到Pattern栏能清楚看对峰的情况 1 2 3 平滑处理 曲线更平滑 可以重新导出平滑数据 薄膜分析及纳米膜的结构分析的实例 Hybrid模块 —— PRS 正比探测器 Different angle bring us different information X ray Nano film Detector Angle of the total X ray reflection The tangent of the curve is connected the scattering information of the nano particle Angle of the total X ray reflection The multi-layer nano structure of poly membranes can be measured The tangent of the curve shows there is SAXS phenomenon in X ray reflectivity test The theory of Small Angle X-ray Scattering Reciprocal space A — Crystallite(grain) B — Particle(primary particle) C — Agglomerate,Aggregate,Flocculate Crystallite、Particle 、Agglomerate A kind of nanometer diamond powder =4.1nm =8.4nm =470nm — XRD — SAXS — C S The comparson of four methods on Determination of Particle Size Distribution of nanometer Powder TEM＋Image Analysis Photon Correlation Spectroscopy (PCS) BET Gas Adsorption Small Angle X-ray Scattering (SAXS) TEM＋Image Analysis Audio-visual,seeing,size,shape and morphology Extremely accurate Authoritative TEM，SEM Computer video-graphy Video-Capture Card Histogram,cumulative plot,mean and median particle size A large n