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The sol-gel transition in gelatin viewed by diffusing colloidal probes.pdf
Polymer Gels and Networks 3 (1995) 407-428
0 1995 Elsevier Science Limited
Printed in Northern Ireland. All rights reserved
0966-7822/95/$09.50
ELSEVIER O!X-7822(94)OOOl2-7
The Sol-Gel Transition in Gelatin Viewed by
Diffusing Colloidal Probes
M. Djabourov, * Y. Grillon J. Leblond
Laboratoire de Physique et MCcanique des Milieux HCtCrogknes, CNRS URA 857,
ESPCI, 10 Rue Vauquelin, 75231 Paris Cedex 5, France
(Received 20 May 1995; accepted 28 July 1995)
ABSTRACT
This paper reports a dynamic light scattering investigation of the sol-gel
transition of gelatin solutions in the presence of latex spheres, which act
as local probes for the viscoelasticity of the medium. The experimental
procedure allows us to define a local gel time related to the size of the
probes. In the sol state and in the gelling solutions, below the gel point,
the dependence of the apparent difision coeficients of the spheres on
correlation times, shows the existence of a fast local diffusion coeficient
and of a slow long-term diffusion coejicient, related to viscosity. The
behaviour of the fast di#usion coejicient during the course of gelation
was quite unexp
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