Combustion synthesis of Co-doped zinc oxide nanoparticles using mixture of citric acidglycine fuels.pdf

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Combustion synthesis of Co-doped zinc oxide nanoparticles using mixture of citric acidglycine fuels.pdf

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Combustion synthesis of Co-doped zinc oxide nanoparticles using mixture of citric acidglycine fuels

C c S a b a A R R A A K C N C C 1 t p h t i t s b t p f C m H s H t f c 3 0 dJournal of Alloys and Compounds 509 (2011) 1915–1919 Contents lists available at ScienceDirect Journal of Alloys and Compounds journa l homepage: www.e lsev ier .com/ locate / ja l l com ombustion synthesis of Co-doped zinc oxide nanoparticles using mixture of itric acid–glycine fuels ousan Rasouli a,?, Shirin Jebeli Moeenb Department of Nanomaterials Nanocoatings, Institute for Color Science and Technology (ICST), 55 Vafamanesh Ave., HosseinAbad Square, Pasdaran St, 1668814811, Tehran, Iran Department of Inorganic Pigments and Glaze, Institute for Color Science and Technology (ICST), 55 Vafamanesh Ave., HosseinAbad Square, Pasdaran St, 1668814811, Tehran, Iran r t i c l e i n f o rticle history: eceived 9 May 2010 eceived in revised form 11 October 2010 a b s t r a c t In this study, cobalt-doped ZnOnanoparticleswere synthesized by combustionmethod.Mixtures of citric acid and glycine were used as fuel. As-prepared powders were characterized by XRD, XPS, SEM-EDX, TEM and spectrophotometer. XRD patterns indicated that combustion reaction by different fuel mixtureccepted 21 October 2010 vailable online 30 October 2010 eywords: hemical synthesis anostructured materials o:ZnO resulted in the formation of pure ZnO phase. However, citric acid combustion alone led to amorphous powder. Scherrer’s equation demonstrated that the crystallite size increaseswith citric acid/glycine (C/G) ratio (38–61nm). SEM and TEM images illustrated that the morphology of the powder depends on the C/G ratios and changes from rod-like to spongy hexagonal particles. Reflectance spectra showed that by higher C/G ratios, deeper green colors are obtained. ? 2010 Elsevier B.V. All rights reserved. olor properties . Introduction There has been increasing interest in ZnO nanostructures due to heir varietyofmorphologies andavailability of simple and lowcost rocessing. Moreover, ZnO remains as a dominant material which olds gr