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Microstructural+evolution+of+Al20Si5Fe+alloy+during+rapid+solidification+and+hot+consolidation.pdf

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MicrostructuralevolutionofAl20Si5Fealloyduringrapidsolidificationandhotconsolidation

RARE METALS V01．28，No．6，Dec 2009,p．639 DoI：10．1007／s12598-009．0122-3 Microstructural evolution of AI·20Si-5Fe alloy during rapid solidification and hot consolidation M．Rajabi8，M．Vahidi8，A．Simchi¨，and P．Davami8 。DepartmentofMaterialsScienceandEngineering，SharifUniversityofTechnology,尸．D．Boxll365-9466,AzadiAvenue．14588Tehran,Iron 6InstituteforNanoscienceandNanotechnology(INST),SharifUniversityofTechnology,P．o．Boxll365．蛳Aza击Avenble,14588Tehran,lran Received 1 1 December 2008；received in revised form 2 March 2009；accepted 5 March 2009 Abstract AI一20Si-5Fb melt was rapidly solidified into particles and ribbons and then consofidated to near full density by hot pressing at 400001250 ma／l h．According to the eutectic—growth and dendritic-growth velocity models．the solidification front velocity and the amount of under- cooling werje estimated for the particles with different sizes．VaiUes of0．43．1．2 cm／s and 15．28 K were obtained．The secondary dendrite a肿 spacing revealed a cooling rate of 6×lo)卧for the particles with锄average size of 20 Inn．Solidificafion models fbfⅡle ribbons yielded a cooling rate of 5×10 7 K／s．As a result of the higher cooling rate．the melt-spun ribbons exhibited considerable microstruetural refinement and modification．The size of the primary slicon decreased from approximately 1 pm to 30 nln while the formation of iron-containing inter- metallic compounds was suppressed．Supersaturation of the aluminum mauix in all amount of～7 at．％Si was noticed from the XRD patterns． During the hot consolidation process，coarsening of the primary silicon particles and precipitation of pAl5Fesi phase were observed．Evalua- tion of the compressive strength and hardness of me alloy indicated an improvement in mechanical properties due to the microstmctural moditication． Keywords：AI··Si-·Fe alloy；rapid solidification；cooling rate；microstructure；mechanical properties 1．Introduction Rapid solidification processes possess some non—equilibrium effects such as microstructure refineme