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PAGE  PAGE 13 辅酶催化法合成安息香 ——辅酶用量对合成安息香产率的影响 ? ? ? 学号：······· 姓名：······· 班级：······· 指导教师：····· 目录 摘要···················································································3 关键词················································································3 第一章 前言·······································································4 1.1实验目的······································································4 1.2主要方法················································??·····················4 1.3产品的用途···································································4 第二章 实验部分 2.1实验仪器及试剂·····························································5 2.1.1实验装置图·····························································5 2,2实验过程和方法······························································6 2.2.1实验过程·································································6 2.2.2计算方法································································7 2.2.3注意事项································································7 第三章 数据处理······························································8 3.1数据记录······································································8 3.1.1 VB1用量和安息香产率·················································8 3.1.2 熔点测定······························································9 3.2 数据处理······································································9 3.2.1安息香产率柱图························································10 3.2.2安息香熔程·····························································10 3.3IR光谱分析···································································11 第四章 结果与讨论·························································11 参考文献···········································································12 摘要：?以苯甲醛为原料，辅酶VB1为催化剂，利用缩合反应制备安息香。本实验采用单因素法，寻求体系在不同辅酶用量时对反应产率的影响：辅酶用量在基准量是1.8g，通过设定1.6g、1.8g、2.0g、2.1g辅酶用量，以15ml苯甲醛，6ml水，15ml 95%的乙醇，150g/L氢氧化钠，pH达到9~10，测定产物的量，证