12 mei liquefaction of loose quality standard.docVIP

 PAGE \* MERGEFORMAT 15 12 mei liquefaction of loose quality standard [Abstract] Objective: To establish a 12 flavored liquid powder quality control standards. Methods: The thin-layer chromatography on the main medicinal preparations TPG, Salvia, Treats, dried tangerine peel for qualitative identification, using HPLC determination of tanshinone Ⅱ A Salvia content. Results: Identification of specific, quantitative method is simple and accurate. Tanshinone Ⅱ A at 5.440 μ g ~ 32.640 μ g was well within the linear relationship (r = 0.999 966 3), the average recovery was 99.99% (n = 5), RSD = 0.3. Conclusion: The quality standards used in method is accurate and reliable, a good feasibility and reproducibility, can effectively control the quality of the preparation. [Keywords:] 12 mei liquefied powder; quality standards; TLC; HPLC; tanshinone Ⅱ A Abstract Objective: To establish the method for quality control of Shi’erwei Yehua Powder.Methods: Radix Paeoniae Rubra, Radix Salviae Miltiorrhizae, Cortex Phellodendri and Pericarpium Citri Reticulatae in Shi’erwei Yehua powder were identified by TLC, the content of tanshinone Ⅱ A in Pericarpium Citri Reticulatae was determined by HPLC.Results: The method of identification was specific, the quantitative method was simple and accurate.The calibration curve showed a good linear relationship in the range of 5.440 μ g ~ 32.640 μ g for tanshinone Ⅱ A, r = 0.999 966 3.The average recovery was 99.99% (n = 5), RSD = 0.3.Conclusion: Two methods are accurate, reliable with good feasibility and repeatability, can be used to control the quality of this powder effectively. Keywords: Shi’er wei Yehua Powder, quality standard, TLC, HPLC, tanshinone Ⅱ A 12 flavored liquid bulk provided by the Shenzhen Municipal Chinese Medicine Hospital, from cork, Ligustrum lucidum, Anemarrhena, to yellow, red peony, red sage root, artillery Shan Jia, Sanleng Ezhu, Bodhisattva, Alisma, dried tangerine peel composed of 12 Chinese herbal medicin