Application of microemulsion in Sophora flavescens and its proprietary Chinese medicines the application of thin layer chromatography analysis of studies.docVIP
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Application of microemulsion in Sophora flavescens and its proprietary Chinese medicines the application of thin layer chromatography analysis of studies
Author: Sun Yue Liang-wang Chen Zhibin Ye built
[Abstract] Objective To investigate the microemulsion thin layer chromatography for the isolation and identification of alkaloids in Sophora flavescens isolation and identification methods, and at the same time with a variety of active ingredients in traditional Chinese medicine Sophora flavescens. Way to sodium dodecyl sulfate - butanol - n-heptane - water micro-emulsion for the launch of agent, in an ordinary silica gel plate was alkaloids in Sophora flavescens Ait microemulsion thin-layer chromatography analysis, examining the various separation conditions on the hard Participation in the separation of alkaloids, and with the traditional TLC methods were compared. On this basis, through a point-like to start with microemulsion thin layer chromatography separation and detection of Sophora proprietary Chinese medicines - in a variety of compound Shi Wei Capsules ingredients. Results are 30% water content for the launch of the micro-emulsion agent, on Sophora Alkaloids have a good separation effect, the alkaloid of the Rf values are within the scope of 0.2 ~ 0.8, this launch agent for the compound Shi Wei Capsules The isolation and identification, which can detect a variety of active ingredients, easy to operate, separating the results are satisfactory, and the detection sensitivity. Conclusion microemulsion thin layer can be used for Sophora Isolation and Identification of medicinal herbs and proprietary Chinese medicines.
[Keywords:] microemulsion thin-layer chromatography compound Shi Wei Capsules Kushen
Abstract: ObjectiveTo investigate the application of microemulsion TLC in separation and identification of alkaloids of Sophara and its patent medicine-Shiwei Compound Capsule. MethodsSodium dodecyl sulphate/n- C4H9OH/n-C7H16/H2O mi
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