Atomic absorption spectrometry of trace elements in renal Ning San zinc capsules.docVIP

 PAGE \* MERGEFORMAT 8 Atomic absorption spectrometry of trace elements in renal Ning San zinc capsules [Abstract] Objective To establish a renal capsule rather casual determination of zinc. Methods HNO3-HClO4 digestion, inductively coupled plasma atomic emission spectrometry (ICP-AES), lamp current: 10 mA, wavelength: 213.8 nm, Slit: 0.3 nm, air flow: 9.4 L / min, acetylene flow rate: 2.0 L / min, combustion head height: 7.5 mm. Results zinc regression equation: Y = 0.054X #8203;#8203;+0.001 1, zinc ion concentration of 0.2 ~ 1.6 μg / mL range was a good linear relationship, r2 = 0.999 3, Shen Ning Powder Capsules average concentration of zinc 68.6 μg / g, the average recovery was 99.56%, RSD = 2.00%. Conclusion The method is simple , reliable, Shen Ning powder capsules can be used as a method of quality control. [Keywords:] kidney capsule rather loose, trace elements, zinc, atomic absorption spectrometry determination Abstract: Objective To establish an ICP-AES method for determination of the content of Zn in Shenningsan Capsules. Methods The sample was digested with HNO3-HClO4, and determined by the ICP-AES method. The determined wavelength was at 213.8 nm, the electric current of the light was set at 10.0 mA, the slit-width was 0.5 nm, the flow rate of acetylerce was 2.0 L / min and the flow rate of air was 9.4 L / min, the hight of burning was 7.5 mm. Results The ion concentration of Zn had the good linear range of 0.2 ~ 1.6 μg / mL, Y = 0.054X #8203;#8203;+0.001 1 (r2 = 0.999 3). The average recovery of the content of Zn in Shenningsan Capsules was 99.56% with RSD of 2.00% . The content of Zn in Shenningsan Capsules was 68.6 μg / g. Conclusion The method is simple and reliable. It can be used effectively for the quality control of Shenningsan Capsules. Keywords:: Shenningsan Capsules, trace element, Zn, ICP-AES, content determination Shen Ning Tsui bulk capsules prescription by the watermelon clothing, drugs such as the composition of garli