Atractylodes and stir fried mixed citrus aurantium CO2 supercritical extraction process analysis and GC-MS analysis.docVIP

 PAGE \* MERGEFORMAT 9 Atractylodes and stir fried mixed citrus aurantium CO2 supercritical extraction process analysis and GC-MS analysis [Abstract] Objective Atractylodes fried and fried citrus aurantium extract mixture of supercritical CO2 extract the best technology and the chemical composition. Methods orthogonal design method to extract pressure, temperature, CO2 flow rate, extraction time factor, study Supercritical CO2 extraction and optimal conditions for GC-MS analysis. Results of supercritical CO2 extraction of the best conditions were: extraction pressure 33 MPa, extraction temperature 40 ℃, CO2 flow rate 27 L / h, extraction time 60 min. from extraction are mainly composed of γ-elemene. Conclusion The extraction of supercritical CO2 extraction technology of Atractylodes fried and fried citrus aurantium, can shorten the extraction time, significantly improve the yield. [Keywords:] fried Atractylodes; fried citrus aurantium, supercritical CO2 extraction, orthogonal design, GC-MS analysis Abstract: Objective To study the optimum parameters of the supercritical CO2 fluid extraction of roasted Rhizoma Atractylodis Macrocephalae and roasted Fructus aurantii immaturus, and chemical constituents of extractive matters. Methods The experiment was performed with orthogonal design. Four factors were extractive pressure, temperature, extractive time and the flow rate of CO2. GC-MS was applied for analyzing. Results The optimum condition were obtained: the extractive pressure was 33 MPa, the temperature of extraction was 40 ℃, the extractive time was 60 minutes and the flow rate of CO2 was 27 L / h. The main chemical constituents was gamma-Elemene. Conclusion The method applied to obtain the extractive matters from roasted Rhizoma Atractylodis Macrocephalae and roasted Fructus aurantii immaturus was quickly and efficiently with satisfactory results. It provides foundation for exploration. Keywords:: roasted Rhizoma Atractylodis Macrocephalae, roasted