Chuanxiong polar characteristic fingerprint.docVIP

 PAGE \* MERGEFORMAT 7 Chuanxiong polar characteristic fingerprint Of: PENG, Fujian Wu, Zhou Yuchun, Huang Liyun [Abstract] Objective To study the polar Chuanxiong high performance liquid chromatography (HPLC) fingerprint method. Ferulic acid as a control method, using Eclipse XDB-C18 (ODS-2, 250 mm 4. 6 mm, 5 m ) column, mobile phase was methanol -1% acetic acid gradient elution, flow rate 1.0 ml / min, column temperature 25 , detection wavelength 298 nm. the results of 10 common peaks were identified, of which 7 ferulic acid peak peak peak of the reference fingerprint. for the fingerprints of the test solution and control all of the fingerprint peaks corresponding to 10, and the same order. Conclusion The method is simple, accurate, and studies of Chuanxiong fingerprint stability, repeatability , and can be used as part of the characteristic polar Chuanxiong fingerprint. [Keywords:] Chuanxiong; fingerprint; high performance liquid chromatography Abstract: ObjectiveTo study the detection methods with fingerprint chromatogram for polar parts of Chuanxiong Rhizome.MethodsWith ferulenol as the reference substance, Eclipse XDB-C18 (ODS-2, 250 mm 4. 6mm, 5m) was used as the chromatographic column.The mobile phase was methanol and 1% HAC, the temprature was 25 , the flow rate was 1.0 ml / min, and the wavelength was 238 nm.Results There were 10 peaks, of which the seventh was the ferulenol peak, the reference peak. The ten peaks also existed in the sample just as in the reference solution, whose order was corresponded. ConclusionThe method is simple and accurate with good reproducibility and stability and can be used as the polar characteristic fingerprint atlas. Keywords:: Chuanxiong Rhizome; Fingerprint chromatogram; HPLC Chuanxiong the Umbelliferae Chuanxiong Ligusticum chuanxiong Hort.’s Dried roots, Qi stagnation and blood stasis due to irregular menstruation, dysmenorrhea, amenorrhea, liver Qi stagnation, blood Erzhi sluggish Xiong Xie pain