Components of The Hills Gastroenterology.docVIP

 PAGE \* MERGEFORMAT 7 Components of The Hills Gastroenterology [Abstract] Objective The Hills Gastroenterology Tujia drug Isolation and identification of components. Methods ethanol soaking, step by step extraction method to extract components The Hills Gastroenterology. Using normal phase, reverse phase silica gel column chromatography, high performance liquid chromatography the method of separation, purification and detection by 13C-NMR spectroscopy, 1H-NMR spectrum of its structural identification. Results Geshanxiao isolated from ethanol extract of 6 Chemical composition: methyl phenol (, sucrose ( , daucosterol (, kidjoranin 3-O-@-L-cymaropyranosyl-(1 4--D-cymaropyranosyl-(1 4 - @-L-diginopyranosyl-(1 4--D-cymaropyranoside ( ,12-O-benzoyllineolon 3-O-@ - L-cymaropyranosyl-(1 4--D-cymaropyranosyl-(1 4 - @ - L-diginopyranosyl-(1 4--D-cymaropyranoside ( , 2,4 Dihydroxyacetophenone (. Conclusion Compounds and for the first time to get from Geshanxiao. [Keywords:] Geshanxiao, chemical composition Drug, also known as the Tujia Cynanchum Geshanxiao is the ear leaf plants dill japonica Cynanchi Cynanchum auriculatu Royle Wight dry roots. Cynanchum have found to enhance immunity, anti-tumor and anti-aging effects [1]. In order to develop use of the medicinal resources, the paper Geshanxiao studied the chemical constituents, and from 6 isolated compounds were identified as: methyl phenol, sucrose, daucosterol, kidjoranin 3-O-@-L-cymaropyranosyl- (1 4--D-cymaropyranosyl-(1 4 - @-L-diginopyranosyl-(1 4--D-cymaropyranoside ,12-O-benzoyllineolon 3-O-@-L-cymaropyranosyl-(1 4--D-cymaropyranosyl-(1 4 - @-L-diginopyranosyl-(1 4--D-cymaropyranoside, 2,4 - Dihydroxyacetophenone. 1 Apparatus and reagents Vafian Mercury VX-300/500 NMR instrument, Diane U3000 semi-preparative high performance liquid chromatography, conventional silica gel and separated by thin layer chromatography silica gel column chromatography by the Qingdao Marine Chemical Plan