Explore gas chromatography Jing Jiang content of cold pills.docVIP

 PAGE \* MERGEFORMAT 8 Explore gas chromatography Jing Jiang content of cold pills [Abstract] Objective: To establish a gas chromatography Jing Jiang cold pills in the content of methyl nonyl ketone. Method: steam distillation for the test materials prepared by solution, nitrogen as carrier gas, detector temperature is 280 ℃ , the column temperature was programmed temperature, inlet temperature of 240 ℃ . Results: In the chromatographic conditions, methyl-nonyl-ketone at 0.024 468 ~ 0.12 234 mg / mL (r = 0.9 996) showed good linear relationship within the framework of the average recoveries were 99.22%. Conclusion: The method is simple, fast, accuracy and repeatability are good, Jing Jiang cold pills can be used for quality control methods. [Keywords:] cold pills; determination; gas chromatography Jing Jiang cold pills prescription main ingredient of Houttuynia, Nepeta and other herbs, to improve its bioavailability to immediate release of the role, be prepared for the pills agent. Upon completion of pills on the basis of the optimum inspection and further improve its determination. Volatile oil is the main efficacy Yuxingcao components containing Decanoyl acetaldehyde, methyl nonyl ketone, lauryl aldehyde and other components, but also for the methyl-nonylketone the main component of volatile oil, the author using gas chromatography Jing Jiang cold pills to methyl-nonyl-ketone determination. An instrument and reagent Shimadzu GC-14C gas chromatograph instrument; JA5103N Electronic Precision Balance (Shanghai Precision Scientific Instrument Co., Ltd. China Bridge); is 11 alkane, purchased in the U.S. Sigma Company, batch number: LB43172; the reagents were pure and analytical HPLC pure. Two chromatographic conditions Shimadzu GC-14C gas chromatograph instrument, the assembly of hydrogen flame ionization detector, column was DB-1 quartz capillary column (30 m * 0.25 mm * 0.25 μ m), injection port temperature 240 ℃ , detector temperature 280 ℃ , Start the i