Gas chromatographyMS determination of the content of camphor Fengyoujing.docVIP

 PAGE \* MERGEFORMAT 3 Gas chromatographyMS determination of the content of camphor Fengyoujing [Abstract] Objective To determine the concentration of camphor Fengyoujing method. Methods using gas chromatography  mass spectrometry methods to naphthalene as the internal standard, SPB  1701 (30 m * 0.25 mm * 0.25 μ m) quartz capillary column; 80 ~ 250 ℃ temperature programming. The results of the volume of naphthalene 2.56 * 10-3 ~ 12.8 * 10-3μ g within the range of the ratio of peak area has a good linear relationship (r = 0.9998), the average recovery was 97.6%, detection limit: 1.3 * 10 -- 3μ g. Conclusion The method is rapid, accurate, sensitive, reproducible, and can be used Fengyoujing preparation quality control. [Keywords:] gas chromatography  mass spectrometry; camphor; Fengyoujing Determination of camphor in Fengyoujing by gas chromatography  mass spectrometry Abstract: Objective To develop a method for the content determination of camphor, the main component in Fengyoujing.Methods Camphor in Fengyoujing was analyzed by gas chromatography  mass spectrometry using naphthalene as internal standard. Camphor and naphthalene were analyzed on a SPB  1701 column with programing temperature from 80 to 250 ℃ . Results The linear range of the method was 2.56 * 10-3 ~ 12.8 * 10-3 μ g with a relative standard deviation of 2.5%. The detection limit of camphor was 1.3 * 10-3 μ g. Conclusion The method is rapid, accurate and reproducible for the quality control of Fengyoujing. Keywords:: gas chromatography; mass spectrometry; camphor; Fengyoujing Fengyoujing mainly by menthol, camphor, methyl salicylate, etc. made of multi-drug coupled with spices, with a special aroma and taste of cold and hot, there are anti-inflammatory, analgesic, cool, itching, Qufeng of efficacy, for cold induced headache, dizziness and joint pain, toothache, abdominal pain and mosquito bites, motion sickness and other discomfort caused by [1], can be used for mild burns, ring