HPLC Determination of Su Kiyomaru the content of baicalin in.docVIP

 PAGE \* MERGEFORMAT 7 HPLC Determination of Su Kiyomaru the content of baicalin in [Abstract] To establish HPLC determination of Su Kiyomaru the content of baicalin. Methods Phenomenex C18 Gemini (250mm * 4.6mm, 5μ m) column, column temperature at room temperature with methanol -0.5% phosphoric acid (50:50) as mobile phase; flow rate of 1.0ml/min; detection wavelength: 280nm. The results of baicalin into the sample volume within the range of 0.501 ~ 2.506μ g peak area showed good linear relationship (r = 0.9999), the average recovery was 99.10%, RSD = 0.50% (n = 5). Conclusion The method is simple and accurate, this product can be used as an effective method of quality control. [Keywords:] HPLC Su Kiyomaru baicalin [Abstract] Objective To establish a HPLC method for the quantitative determination of Baicalin in Suqing pills.Methods The determination was performed on Phenomenex C18 column (250mm * 4.6mm, 5μ m) with the mobile phase consisted of methanol-0.5% phosphoric acid solution ( 50:50) and the column temperature was ambient. The flow rate was 1.0ml/min.The detection wavelength was set at 248nm.Results The method showed a good linear relationship within the range of 0.501 ~ 2.506μ g of Baicalin (r = 0.9999 , n = 5). The average recovery rate was 99.10% with RSD = 0.50% (n = 5). Conclusion The method is simple and accurate and can be used for the quality control of Suqing pills. [Keywords:] HPLC; Suqing pill; baicalin Su-qing Pills by Poria, baicalin, berberine, the Health plantago-jen 9 taste, etc. Prescription medicines made of Chinese medicine hospital preparation room for the Lianyungang preparations for the heat dampness, attending intrinsic hot and humid, mouth pain, dry mouth, sticky mouth do not think diet, mental fatigue, bowel unhappy, and thick yellow tongue coating, clinical use heat Xiehuo, anti-inflammatory to facilitate the results remarkable. In order to ensure quality of preparation, the author according to Fang ingredients, select one