Participation White Pills on the establishment of quality standards.doc

 PAGE \* MERGEFORMAT 10 Participation White Pills on the establishment of quality standards Study: http Zhang, Yu Dan, are Xiaowei, TRADITIONAL, Liu Yaping, Yan Mei [Abstract] Objective To establish the quality standards Shenbai Pills. Methods of thin layer chromatography preparations were in the astragalus, red peony, and Rhizoma Imperatae qualitative identification, the use of the main active ingredient HPLC method to determine the content Sal B. Results Participation White Pill in Astragalus, Radix and Rhizoma Imperatae by TLC spots were clear and reproducible, non-interference of placebo, HPLC method assay results showed that Sal B, the average recovery was 99.74% (RSD = 2.08%), precision RSD = 1.74%, repeatability of RSD = 1.19%, the stability of RSD = 1.70%. Conclusion The method is simple, accurate, stable, and can be used as reference standards for quality control of White Pills . [Keywords:] White Pills parameters, quality standards, TLC, HPLC Abstract: Objective To set up the quality standard of Shenbai concentrated pills. Methods Radix Astragali, Radix Paeoniae Rubra and Rhizoma Imperatea in Shenbai concentrated pills were identified with the method of TLC. The concentration of salvianolic acid B was determined with the method of HPLC. Results For TLC, the chromatogram spots of Radix Astragali, Radix Paeoniae Rubra and Rhizoma Imperatea were well separated and without interference in their negative controls. Quantitative analysis of HPLC showed that the average recovery of salvianolic acid B was 99.74% (RSD = 2.08%) with the RSD of precision, reproducibility and stability was 1.74%, 1.19% and 1.70%, respectively. Conclusions The methods set up by this study are easy, accurate and stable, and can be used as the quality control standard of Shenbai concentrated pills. Keywords:: Shenbai concentrated pills, quality standard, TLC, HPLC Participation White Pill white soup is clinically effective parameters based compound developed by tr