Qing Feng Teng chemical constituents of.doc

 PAGE \* MERGEFORMAT 9 Qing Feng Teng chemical constituents of Author: Ban built a small red, yellow, Yan Li Yan Zhou Lan Zhang Jiming YANG Xiao-Sheng Zhang Yuan-Hu [Abstract] Objective To Green acutum chemical constituents were isolated and identified. Methods silica gel column chromatography, RP-Rp  18 column chromatography and recrystallization methods such as separation and purification, combined with 1H  NMR, 13C  NMR, EI  MS and identified by physical and chemical constants. The results from the Green acutum 95% ethanol extract of isolated and identified six compounds were identified as: sinomenine ① , daucosterol ② ,(-)- DL-syringaresinol ③ , syringaresinol-4 ‘, 4’-O-bis - β -D-glucoside ④ , syringin ⑤ , ()-syringaresinol-4’-O-β -D-monoglucoside ⑥ . Conclusion Compounds 4,5 for the first time from the Green acutum isolated and identified. [Keywords:] Qing Feng Teng chemical composition of Abstract: ObjectiveTo study the chemical constituents in the stems and rhizomes of Sinomenium acutum. Methods Column chromatograghy on Silica gel, Rp  18 and recrystallization were applied for the isolation and purification of the constituents.The structures were elucidated by their physicochemical properties and spectral data.ResultsSix compounds were obtained and identified as sinomenine ① , daucosterol ② , (-) -DL-syringaresinol ③ , syringaresinol  4 ‘, 4’-O-bis-β -D-glucoside ④ , syringin ⑤ , ()-syringaresinol-4’-O-β -D-monoglucoside ⑥ . ConclusionCompounds 4,, 5 were isolated from this plant for the first time. Keywords:: Sinomenium acutum; Chemical constituent Green Wind rattan for Menispermaceae plant ivy Sinomenium acutum (Thunb.) Rehd. Et Wils. And hairy ivy S. acutum (Thunb.) Rehd. Et. Wils. Var. Cinereum Rehd. Et Wils.’s Dry vine stems, There rheumatism, the flow of qi, Lee urine of efficacy for the treatment of rheumatism Bi Tong, joint swelling, numbness itching embolism. The plant mainly contains alkaloids [1 ~ 3]. As the composition of