Scorzonera mongolica volatile oil components and inorganic elements in GC MS and ICP MS analysis.docVIP

 PAGE \* MERGEFORMAT 16 Scorzonera mongolica volatile oil components and inorganic elements in GC MS and ICP MS analysis 【Abstract】 Objective To study the Mongolian Scorzonera Scorzonera mongolica Maxim. Volatile oils and inorganic elements of the composition and relative content. Methods Soxhlet extraction method Scorzonera mongolica volatile oil extracted by microwave digestion are inorganic elements in the sample. Using GC / MS and ICP / MS for their volatile oils and inorganic elements for analysis. The results identified 13 types of volatile oil components, accounting for 93.43% of the total volatile oil, were first reported; determination of 27 inorganic elements, element content of the order: Ce, K, Al, Ca, Fe, La, Mg, Na, P, Ga, Mn, Ba, Zn, B, V, Cr, Cu, Ni, Pb, Th, As, Co, Se, Sr, Mo, Cd and Hg. Conclusion of two main components of volatile oil of 31 alkanes (34.75%), and Ho Pa -22 (29) - ene-3β-ol (21.47%), accounting for 56.22% of the total volatile oil. 27 inorganic elements Ce, K, Al, and Ca content, and trace elements Ce, Ga, Mn, and Zn higher levels. Keywords: Scorzonera mongolica inorganic elements in volatile oil GC-MS chromatography inductively coupled plasma mass spectrometry Analysis of Volatile Oils and Inorganic Element of Scorzonera mongolica Maxim. By GC  MS and ICP  MS Abstract: ObjectiveTo study the volatile oils and inorganic elements of Scorzonera mongolica Maxim. MethodsVolatile oils of Scorzonera mongolica Maxim. Were extracted by Suo recovery (hot refluxing) method and analysed by GC  MS. Sample of inorganic elements was digested with microwave digestion system and measured by ICP  MS.Results13 constituents of volatile oil were determined, and identified up to 93.43% of the constituents. 27 kinds of inorganic elements were determined, they were Ce, K, Al, Ca, Fe, La, Mg, Na, P, Ga, Mn, Ba, Zn, B, V, Cr, Cu, Ni, Pb, Th, As, Co, Se, Sr, Mo, Cd and Hg. ConclusionThe main components of volatile oil