One-Pot and Efficient Synthesis of Triazolo[1,2-a]indazole-triones via Reaction of Arylaldehydes with Urazole and Dimedone Catalyzed by Silica Nanoparticles Prepared from Rice Husk 英文参考文献.docVIP

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One-Pot and Efficient Synthesis of Triazolo[1,2-a]indazole-triones via Reaction of Arylaldehydes with Urazole and Dimedone Catalyzed by Silica Nanoparticles Prepared from Rice Husk 英文参考文献.doc

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One-Pot and Efficient Synthesis of Triazolo[1,2-a]indazole-triones via Reaction of Arylaldehydes with Urazole and Dimedone Catalyzed by Silica Nanoparticles Prepared from Rice Husk 英文参考文献

Molecules 2011, 16, 9041-9048; doi:10.3390/moleculeOPEN ACCESS molecules ISSN 1420-3049 /journal/molecules Article One-Pot and Efficient Synthesis of Triazolo[1,2-a]indazole- triones via Reaction of Arylaldehydes with Urazole and Dimedone Catalyzed by Silica Nanoparticles Prepared from Rice Husk Hooshang Hamidian 1,*, Samieh Fozooni 2, Asadollah Hassankhani 3 and Sayed Zia Mohammadi 1 1 Department of Chemistry, Payame Noor University (PNU), P.O. Box 19395-369776175-559, TehranKerman, Iran; E-Mail: szmohammadi@ (S.Z.M.) 2 Mining and Engineering Department of Zarand, Shahid Bahonar University, Kerman, 76169-14111, Iran; E-Mail: s_fozooni@ (S.F.) 3 Department Institute of Materials Environmental Science, International Center for Science and High Technology and Environmental Science, P.O. Box 76315-117, Kerman, Iran; E-Mail: ahassankhani@ (A.H.) * Author to whom correspondence should be addressed; E-Mail: hooshanghamidian@; Tel.: +98-341-3342451; Fax: +98-341-3342451. Received: 19 September 2011; in revised form: 13 October 2011 / Accepted: 20 October 2011 / Published: 26 October 2011 Abstract: A novel synthesis of triazolo[1,2-a]indazole-1,3,8-trione derivatives by reaction of urazole, dimedone and aromatic aldehydes under conventional heating and microwave irradiation and solvent-free conditions using silica nanoparticles prepared from rice husk ash as catalyst is described. The new method features high yields, multicomponent reactions and environmental friendliness. Keywords: multicomponent reaction; nanosilica sulfuric acid; microwave irradiation; rice husk 1. Introduction Rice husk is an abundantly available material rich in silica. It is a large-volume waste product of the rice milling industry in rice producing countries. New studies have produced silica nanoparticles from rice husk [1-3]. In recent years, silica nanoparticles have gained importance in scientific research due Molecules 2011, 16 9042 to th