Role of SAM Chain Length in Enhancing the Sensitivity of Nanopillar Modified Electrodes for Glucose Detection 英文参考文献.docVIP
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Sensors 2009, 9, 1295-1305; doi:10.3390/OPEN ACCESS
sensors
ISSN 1424-8220
/journal/sensors
Article
Role of SAM Chain Length in Enhancing the Sensitivity of
Nanopillar Modified Electrodes for Glucose Detection
Venkataramani Anandan 1, Rajan Gangadharan 1 and Guigen Zhang 1, 2, 3, 4*
1 Micro/Nano Bioengineering Lab and 2 Faculty of Engineering, The University of Georgia
3
Bioengineering, Electrical Computer Engineering, Clemson University, 4 Institute for Biological
Interfaces of Engineering, Clemson University
E-mails: vanandan@; rgangad@; guigen@
* Author to whom correspondence should be addressed; Bioengineering, Electrical Computer
Engineering, Clemson University, 401 Rhodes Engineering Center, Clemson, SC 29634, USA
Received: 27 January 2009; in revised form: 24 February 2009 / Accepted: 24 February 2009 /
Published: 26 February 2009
Abstract: In this report, alkanethiol self assembled monolayers (SAM) with two different
chain lengths were used to immobilize the functionalizing enzyme (glucose oxidase) onto
gold nanopillar modified electrodes and the electrochemical processes of these
functionalized electrodes in glucose detection were investigated. First, the formation of
these SAMs on the nanopillar modified electrodes was characterized by the cyclic
voltammetry and electrochemical impedance spectroscopy techniques, and then the
detection sensitivity of these functionalized electrodes to glucose was evaluated by the
amperometry technique. Results showed that the SAM of alkanethiols with a longer chain
length resulted in a higher degree of surface coverage with less defect and a higher electron
transfer resistance, whereas the SAM of alkanethiols with a shorter chain length gave rise
to a higher detection sensitivity to glucose. This study sheds some new insight into how to
enhance the sensing performance of nanopillar modified electrodes.
Keywords: Gold nano
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