水热条件对铜镍微米复合材料超级电容比容量 的影响.pdfVIP

Advances in Material Chemistry 材料化学前沿, 2017, 5(1), 11-24 Published Online January 2017 in Hans. /journal/amc /10.12677/amc.2017.51002 Impact of Hydrothermal Conditions on Copper-Nickel-Micron Composite Ultra Capacitor Specific Capacity 1 2,3* 2 2,3 Chaohui Li , Xiuxia Zhang , Qianyu Ji , Ron Fang 1 School of Material Science and Engineering, Beifang University of Nationalities, Yinchuan Ningxia 2 School of Electrical and Information Engineering, Beifang University of Nationalities, Yinchuan Ningxia 3 School of Optoelectronic Information Engineering, Hefei University of Technology, Hefei Anhui th nd th Received: Jan. 6 , 2017; accepted: Jan. 22 , 2017; published: Jan. 25 , 2017 Abstract Nickel oxide/copper oxide composites are prepared by using cupric chloride and nickel chloride as raw material by chemical reaction with sodium hydroxide to prepare copper hydroxide and nickle hydroxide precipitation which then transferred into autoclave, and calcined. The as- prepared composites were well analyzed by XRD and SEM and the electrochemical performance was investigated by cyclic voltametry, AC impedance and galvanostatic charge-discharge. The re- sults show that under the condition of 150˚C 30 h, the electrochemical performance is the best. The specific capacitance was 200 F∙g−1 at the charge-discharge current of 1 A∙g−1. Keywords Hydrothermal Method, Nickle Oxide, Copper Oxide, Specific Capacity 水热条件对铜镍微米复合材料超级电容比容量 的影响 1 2,3* 2 2,3 李超辉 ，张秀霞 ，冀千瑜，樊 荣 1北方民族大学材料科学与工程学院，宁夏 银川 2北方民族大学电气信息工程学院，宁夏 银川 3合肥工