废弃电路板中环氧树脂真空热解规律的研究_吴倩.pdfVIP

DOI :10.15985/.cnki.1001 -3865.2008.12.004 　　 废弃电路板中环氧树脂真空热解规律的研究＊ # 吴　倩　丘克强 　湛志华 (, 　4 10083) 　　　, 。(200 ～ 700 ℃)、(5 ～30 ℃/min)、(, 3 ～30 kPa)(10 ～ 150 min)。 , ;(400 ～550 ℃)、(15 ～20 ℃/min)、(15 kPa) (30 min)。 　　　　　 Study on vacuum pyrolysis discipliarian of epoxy resin contained in waste printed circuit boards 　Wu Qian, Qiu K eqiang , Z han Z h ihua .(S chool of Ch emis try and Ch em ica l E ng in eer ing, Centra l S ou th Un iversity , Chang sha H u- nan 410083) Abstract:　The effects of pyrolysis con itions on the pro ucts yiel of epoxy resin in w aste printe circuit boar s were investigate with the pyrolysis oven heate by temperature controller.The effect of pyrolysis terminal tempera- ture(200-700 ℃), heating rate(5-30 ℃/min), pressure(3-30 kPa)an hol ing time (10-150 min)on the yiel of vacu- um pyrolysis pro uct w ere analyze .Experimental results showe that pyrolysis terminal temperature was the key factor uring the vacuum pyrolysis process.The optimal con ition w as obtaine as follow s:pyrolysis terminal tem- perature at 400-550 ℃, heating rate of 15-20 ℃/min, pressure of 15 kPa, hol ing time of 30 min. Keywords:　vacuum pyrolysis;w aste printe circuit boar ;epoxy resin 　　, 。, , , 。, 。 ,、。 , [1-7] 、、() , , 、 , ,。 。 ( 1　 ), 1.1　实验样品及成分分析 ,。, 　　 。FR4 ( 。 ), 1 cm×1 cm 。 ,, 1。 , 1.2　实验装置与实验方法 , , 1。-20 ℃ “”, , (NaCl )。 , , ,(), 1 100 ℃, 13 cm,4 cm。