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低温苯甲醇醇解法制备高活性锐钛矿型纳米晶TiO 2 光催化剂 - 复旦大学
27 2 2006 2
Vol.27 o.2 ChineseJournal of Catalysis February 2006
:0253-9837(2006)02-0171-07 :171~177
TiO
2
朱 建, 杨 俊, 陈 麟, 曹 勇, 戴维林, 范康年
(复旦大学化学系, 上海市分子催化与创新材料 点实验室, 上海 200433)
: TiCl , TiO , X 、-
4 2
、、、- 、
2
、, .,
TiO , 、、
2
.400 ℃3 h TiO , Degussa P-25 TiO .
2 2
:;;;;;;
:O643/X7 :A
Preparation of Highly Photoactive Nanocrystalline Anatase TiO2
by Low-Temperature Benzyl Alcohol Alcoholysis
ZHU Jian, YANG Jun, CHEN Lin, CAO Yong, DAI Weilin, FAN Kangnian *
(Dep artment of Chemistry and Shanghai Key Laboratory of Molecular Catalysis and Innovative Materials,
Fudan University, Shanghai 200 33, China)
Abstract:A novel low-temperature approach based on benzyl alcohol alcoholysis has been developed to synthesize
the nanocrystalline anatase TiO photocatalyst with a high surface area.The catalysts were characterized by
2
X-ray diffraction, thermal gravimetric-differential thermal analysis, transmission electron microscopy, Raman
spectroscopy, diffuse reflectance UV-Vis spectroscopy, and 2 adsorption.The results showed that calcination
temperature and calcination time had aprofound influenceon the microstructural properties as well as the activity
of the nanocrystalline TiO for photocatalytic degradation of phenol.The as-prepared fresh TiO samplewas con-
2
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