反相高效液相色谱法测定接骨胶囊中阿魏酸的含量论文.docVIP

　　反相高效液相色谱法测定接骨胶囊中阿魏酸的含量论文 .freelm×250 mm,5 μm),流动相为甲醇-1%冰乙酸(33∶67),检测波长为320 nm,流速为1.0 mL/min。结果 阿魏酸在0.12～1.2 μg范围内呈良好的线性关系(r＝0.999 9),平均回收率为99.6%,RSD＝1.8%。结论 该方法简便、准确,可用于控制接骨胶囊制剂的质量。 【关键词】 接骨胶囊；阿魏酸；高效液相色谱法；含量测定 Abstract：Objective To establish a method for determination of Ferulic acid in Jiegu Capsule. Method The samples ined by RP-HPLC on a Hypersil C18 column (4.6 mm×250 mm, 5 μm). The mobile phase consisted of methanol and 1% acetic acid (33∶67). The detection and the floL/min. Results The calibration curves of Ferulic acid L (r＝0.999 9). The average recovery ethod is simple and accurat