基于响应面分析法的超声波洗涤羽毛纤维工艺条件优化.pdfVIP

第 33 卷第7 期 纺织学报 Vo l. 33 , No.7 2012 年7 月 Joumal of Textile Research }ul. , 2012 文章编号:0253-9721(2012)07-0024-07 基于晌应面分析法的 超声波洗涤羽毛纤维工艺条件优化 赵玉萍1 ，张占百1 ，郭雅琳2 ，赵明l (1.大连工业大学绿色纤维材料应用技术研究所，辽宁大连 116034; 2. 辽宁出入境检验检疫局，辽宁大连 116036) 摘 要 通过洗涤降低羽毛纤维上含菌量是其前处理的重要任务。以洗涤时间、洗涤温度、浴比和酸性蛋白酶用 量为自变量，洗净羽毛纤维上嗜温性需氧菌含量为响应值，采用响应面分析法对羽毛纤维的洗涤工艺条件进行优 化。通过单因素试验、Box-Benhnken 中心组合试验和响应面分析法研究各自变量及其交互作用对含菌量的影响， 得到二次多项式回归方程的预测模型，确定超声波洗涤羽毛纤维的最佳工艺条件为:双氧水浓度5mνL， pH 值 4.0 甸 6.0 、洗涤时间20 min 、洗涤温度60 c、浴比1:40 、酸性蛋白酶用量 3% (o.w. f)。按此最优工艺条件洗涤后，羽 毛纤维上嗜温性需氧菌的含量为 3.73 x 10 cfu/g。 关键词 羽毛纤维;超声波z 洗涤:响应面分析法:优化E 嗜温性需氧菌 中图分类号:TS 102.3 文献标志码:A Process optimization of ultrasonic washing of feather flbers based on response surface method 1 1 2 1 ZHAO Yuping • ZHANG Juan , GUO Yalin , ZHAO Ming (1. Green Fiber Application Technology Research lnIJ titute , Dalian Poly臼chnic University , Dalian , Liaoning 116034 , China; 2. Liaoning Entry-Exil Jnspect iDns and Quarantine Bureau , Ðalian , Liaoning 116036 , China) Abstract It is the important task in pretreatment to reduce bacterial content of feather fibers by washing. Process optimization of ultrasonic washing of feather fibers was performed by response surface method in which washing time , washing temperature , liquor ratio and dosage of acid protease were used as independent variables and the mesophilic aerobic bacterial content of feather fibers was used as the