甲基丙烯酸的开车方案(国外英语资料).docVIP

甲基丙烯酸的开车方案 Starting steps I. current status (late stage of methanol through transportation): 1 boiler, air separation, circulating water and chilled water system operate normally; 2. The level of each tower and reflux tank is normal. The temperature, pressure, flow rate, liquid level and other instruments are checked accurately and displayed normally; 3. The pump runs normally and the inlet screen is clean; 4, through the methanol intermodal drills, operators have been able to master DCS and external operation; 5, a step into the molten salt according to heating, heating up to 350~380? C, the normal operation test of molten salt system, hot melt salt discharged into molten salt tank reactor, natural cooling; 6. Once the catalyst is loaded, the purge air is blown continuously and kept dry. Two and two counter unit feeding test (1) methanol cycle: first, the methanol is pumped from the tank farm to the boundary area by methanol, After MOH2025 MOH2010 MOH 2004-50, M1E MMA-2019 MAR 2004-40 M1E MMA2022 to MAR1010 (cross line) R-201 open loop mixing, 24 hours after sampling, such as methanol is polluted by V-221 - C-220 - V-320 (E-310 C-220, MOHs vice line, 2201-65 M1B, LV2202 MOH, 2202-65 M1B, MOH 2203-65 M1B, MOH 3105-65 M1B-PP, MOH 3106-65 M1B, V-320), empty, re injection by V-202 fresh methanol cycle; (2) until the methanol is qualified, the liquid level of R-201/A and D is reduced to 80%, the manhole is opened and the amount of catalyst is added, and the circulation system is debugged. (two filter system operation method). After the filtration system is functioning properly, proceed to the start step. Three, preparatory steps 1, all involved in water transport towers, containers, heat exchangers, intermediate tanks, pipes, instrument systems put aside the net storage water (except C-330), including 200 systems (except C-220), outside the methanol pipeline dry with purified air; 2 all containers, intermediate tanks and tower bottom manholes shall be opened (except C-3